Avance Beginners Guide
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Index
Glossary
Contents
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Contents
Contents
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Introduction
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Sources of Hazards
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Software Version and Command Syntax
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Safety
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Magnetic Safety
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Cryogenic Safety
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Electrical Safety
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Chemical Safety
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CE Certification
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Introductory Theory and Terminology
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NMR Analysis of Chloroform
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Reference Compounds, Hertz, ppm
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Proton NMR - Chemical Shift
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Proton Spectrum of Benzene
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Proton Spectrum of Benzylacetate
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Proton Spectrum of Ethylbenzene with Spin/Spin Coupling
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Decoupling
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FID and Spectrum
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System Description
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AVANCE Architecture Overview
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Operator Console and Connections
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Console
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Link between the Host Computer and the IPSO
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Magnet, Shim System, HPPR and Probe
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The Magnet and Magnet Dewar
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Room Temperature Bore
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Helium Tank
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Nitrogen Tank
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Introduction to the Lock System
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Probes
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Broadband Probe
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Changing a Probe
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Basic Procedures
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The TopSpin Window
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Creating a New Data Set
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Sample Preparation
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Inserting the Sample plus Spinner into the Magnet
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Locking the Sample
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Tuning and Matching the Probe
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Probes Equipped with ATM using the Automated Tuning Routine
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Probes Equipped with ATM Using the Manual Tuning Routine
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Spinning the Sample
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Shimming
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Routine Shimming Using TopShim
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Setting the Probe/Solvent Dependent Parameters
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Adjusting the Receiver Gain
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Starting the Acquisition
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Processing the Data
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Preparing for Acquisition, Frequency Related Parameters
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Frequency
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Numerical Explanation of Transmitted, Basic and Offset Frequencies
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The NMR Sample
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Solvent Selection
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Sample Tube
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Sample Handling
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Proton Spectrum
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Obtaining the Proton Spectrum
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Optimizing the Sweep Width
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Integration
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Plotting the Proton Spectrum
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13C Spectrum with Proton Decoupling
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Obtaining the 13C Spectrum
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Peak Picking
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Plotting the 13C Spectrum
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Basic Troubleshooting
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Contact
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List of Figures
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List of Tables
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Glossary
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Index