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Proton SpectrumObtaining the Proton Spectrum
 
 
Obtaining the Proton Spectrum
The principal steps are described in the Basic Procedures chapter and are as follows:
1. Create a new data set.
 Proton Dataset Window
Note: The directory (DIR) is specific to how the data are stored and therefore may show different entries as the one in the figure above. Click on the down arrow button to browse for a specific directory.
2. Sample preparation.
3. Insert the sample plus spinner into the magnet.
4. Locking the sample.
 Solvents Table
Note: Select DMSO from the solvents table by clicking on it.
5. Tuning and matching the probe.
6. Spinning the sample.
7. Shimming.
8. Setting the probe/solvent dependent parameters.
9. Adjust the receiver gain.
10. Starting the acquisition.
11. Processing the data.
 Processed Proton Spectrum
Further information
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Optimizing the Sweep Width