Home Prof. Newcomb Research Group Research Projects Facilities Publications
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Our research group has access to a wide range
of instrumentation. In addition to the excellent facilities in the
department and university, we operate a number of instruments in the group.
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Laser Flash Photolysis Our laser flash
photolysis units are employed in various kinetic studies. The unit
shown here is our old nanosecond kinetic unit. The laser is in the
back, and from right to left are the UV-vis flash lamp, the reaction
chamber, the monochromator, the photomultiplier tube, and the
oscilloscope. The entire unit is controlled by computer.
This unit can be used for studies of reactions with millisecond to
nanosecond lifetimes. A newer nanosecond unit has the same
capabilities and also incorporates a stop-flow mixing unit for
stopped-flow kinetic studies and "stopped-flow mixing, laser initiated"
kinetic studies. Faster processes are studied with a picosecond
laser kinetic unit. |
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GC and GC-MS
One of the GCs and the GC-MS are shown at the right. The GCs are
automated with a 100 carousal injector, but nobody uses it. The
GC-MS features Chemical Ionization in addition to EI. |
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Spectroscopy
A state-of-the-art diode array UV-visible spectrometer is shown here.
It is the small unit on the right of the picture. In addition to
standard spectroscopy, the spectrometer includes a stopped-flow mixing
unit that allows sub-second mixing and kinetic studies. The
kinetic capabilities of the spectrometer complement the fast
stopped-flow kinetic capabilities of the larger laser flash,
stopped-flow spectrometer and offer the advantage of providing the entire
spectrum in sub-second temporal resolution. |
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This site was last updated
03/19/05
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