Techniques of Optical Spectroscopy in
Analytical Chemistry
(CHEM 524)
Department of Chemistry
Spring Semester, 2013,
Lecture: 170 SES, 2-3:30 pm Tu-Th
Occasional Extra Session: 4342
SES on Wed, 9 or 12,
(These will be demos, problem or review sessions, 2
sections: distribute yourselves)
Professor:
Tim Keiderling
Best
contact: e-mail: tak@uic.edu
Keiderling Group Web Site link (may be of use some day): http://www.chem.uic.edu/takgroup/
Warning
- this site is typically under continuous re-construction by a
non-expert!!
I suggest returning to
look at these html files for periodic review, since I tend to update lextures right before giving them, also the html files for
figures are all operative as links, view best on line and do not print well
However pdf files, can be usefully printed
Please click on these to see the associated files/handouts:
Syllabus for 2013 - rules, outline,
grading
Presentation assignment - sales pitch for
an instrument
Homework
assignments (will
be filled in gradually): #1, #2, #3, #4,
Homework
solutions (just partial sets as available!): #1, #2, #3, #3 extra
Old
Exam models Hour02, Hour05, Hour09, Quiz, Hour11,
Final02,
Final05, Final09,
Final11
Formula
list for the
exams (will be provided for in-class exams)
2013 - Hour Exams and Key:1st Hour
Exam, Answer
Key
EXTRAS:
Links to other Web Pages on
the internet, many company sites, as called out in the notes below
Reference
books on reserve in Library
Lecture notes here in order, below
find links to outside sets of tutorials, notes, presentations etc.:
1. Notes 1
Introduction
2. Notes 2
Conventional light sources
3. Laser
Sources
a. Notes 3a,
Gas lasers
b. Notes 3b
Solid state Laser
4. Notes 4 Optics
5. Notes 5 Special
optics, polarizers, modulators
6.
Notes 6 Monochromators
7.
Notes 7 Interferometers
8.
Notes 8, Detectors
9.
Notes 9, Electronics
10. Notes 10,
Signal to noise
11. Notes 11, Error, statistical treatment
12. Notes 12
Atomic Spectroscopy
13. Notes 13
Molecular spectroscopy
14. Notes 14
Absorption (uv-vis)
15. Notes 15 Fluorescence, Luminescence
16. Notes 16 IR
-(in IR : near IR)
17. Notes 17, Raman
18. Notes 18
Circular Dichroism
19.
Notes 19 DLS etc.
Extra Material:
1. Source
extras
2. Laser
handouts
a. Laser Survey RP Encyclopedia+link
c.
RP gas laser summary article
with links
3. Handouts
for Notes 8, Detectors
a. PMT
b. IR
4. Handout
for Notes 9
5. Slides
for Notes 13
a. General spectroscopic principles
6. Slides
and extra for Notes 15
b. Slides-fluorescence examples
7. Slides
from SAS presentations on IR developments, for Notes 16
a. Sec.1-inst+ATR ,
b. Sec.2-depth+image,
c. Sec.3-kinetic,
8. Extra
from Notes 17, Raman
a. Henry Buijs early
review FT-Raman
b. Renishaw
FT- Dispersive Raman comparison
d. PerkinElmer top 20 Questions
e. Raman of Bio samples--Horiba
9. Extras
for Notes 18, CD
Old notes, links failed, stopped updating mid
semester
Lecture
Notes were moved
from html (in 2009) into a pdf version with integral figures and links,
PDF versions for 2011/13 are in italics and are blue
when recent update links are operative
(The html versions from 2005 have links to figures, which may be of
interest to you, and are pretty complete, but often have distracting strange characters.
You can also go to the older 2005 Web page or
to the very similar 2009 Web
Page)
1: Introduction, basic principles (pdf)
- (2005
html version) - slides- on
spectral methods, light properties
2: Light sources, conventional - (2005 html version)
Links: - Oriel hand out (souces
/optics sections -
radiation
laws)
3: Laser light sources
-
(2005 html version)
Links:
– Laser
Survey RP Encyclopedia+links
-
RP gas laser summary article with links –
b. Solid State, dye and diode lasers
4:
Optics: mirrors and lenses- (2005
html version)
5: Special Optics - (2005
html version)
6:
Monochromators -
(2005
html version)
7:
Interferometers- (2005
html version)
8:
Detectors- (2005
html version)
9:
Signal Processing -
(2005
html version)
10:
Signal to Noise Considerations- (2005
html version)
11: Error, statistical sampling - (2005
html version)
12:
Atomic Spectroscopy - (2005
html version)
13:
Molecular Spectroscopy - (2005
html version)
14:
Absorption Spectroscopy - (2005
html version)
15:
Luminescence Spectroscopy - (2005
html version)
16: Infrared Spectroscopy - (2005
html version)
17:
Raman Spectroscopy - (2005
html version)