A list of some of the available SSNMR experiments

1D Experiments

• 1h.1p9 - single pulse proton
• c13_dec.1p9 - ¹³C single pulse with tppm15 proton decoupling
• cpmas_20k.1p9 - ¹³C CPMAS optimized for spinning at 20 kHz
• cpmas_c90.1p9 - ¹³C CPMAS with flip-back pulse for calibrating ¹³C 90 time 90_CAL
• nqs_vr20k.1p9 - ¹³C non-quaternary suppression optimized for 20 kHz spinning, see only the quats NQS
• cppi_8k.1p9 - ¹³C CPMAS with polarization inversion; CH = null; CH2 = negative; C = positive; CH3 = positive (attenuated however); spin 8 kHz CPPI
• multicp.1p9 - ¹³C quantitative CPMAS reference
• dipinept.1p9 - ¹³C rapid acquisition (50ms D1) with dipolar inept for paramagnetically doped materials reference
• li7.1p9 - ⁷Li
• b11_dec.1p9 - ¹¹B single pulse with tppm15 proton decoupling
• f19.1p9 - ¹⁹F single pulse Tuning_setup
• kbr.1p9 - ⁷⁹Br (for setting Magic Angle) MA
• cpmas_gly.1p9 - ¹³C CPMAS used to set decoupling and cpmas conditions on Glycine OPT
• hahnecho.1p9 - 90-tau-180-tau sequence for eliminating deadtime and baseline roll
• adam_c13.1p9 - ¹³C single pulse on Adamantane, set ¹³C 90 times, shimming and reference ADA
• adam_h1.1p9 - ¹H single pulse on Adamantane, set ¹H 90 times and reference ADA

2D Experiments

• dipinept2d.1p9 - ¹³C/¹H correlation having rapid acquisition (50ms D1) via dipolar inept for paramagnetically doped materials reference
• b11_mqmas_echo.1p9 - MQMAS ¹¹B-isotropic ¹¹B-anisotropic correlation. Split-t1 with shifted-echo acquisition (ie no shearing needed in processing) MQMAS
• b11_mqmas_zfil.1p9 - Basic 3-pulse MQMAS with z-filter for ¹¹B. Shearing (xfshear) is needed in processing MQMAS
• fslghetcor.1p9 - HETCOR ¹H/¹³C-correlation with Lee-Goldburg decoupling. Similar information to the HMQC. Vr=20kHz HETCOR
• cpinad_refoc.1p9 - Refocussed INADEQUATE for unlabelled sample. Vr=20kHz reference eDROOPY phase_cycle
• cpinad_zfr.1p9 - Z-filtered and Refocussed INADEQUATE for labelled and unlabelled sample. Vr=20kHz reference eDROOPY phase_cycle
• wdqsq.1p9 - H/H DQ/SQ correlation with windowed acq, PMLG dec, and PC7 pumps. Vr=12.5kHz and NS=16 reference cramps_2d phase_cycle phase_pc7
• wdqsq64.1p9 - H/H DQ/SQ correlation with windowed acq, PMLG dec, and PC7 pumps. Vr=12.5kHz and NS=64(better selection) reference cramps_2d phase_cycle
• wpmlg2_hhcorr.1p9 - H/H SQ/SQ correlation with windowed acq, mix time 500us etc; Vr=12.5kHz and NS=16 reference distances cramps_2d
• hn_hmqc.1p9 - 1H/14N 2D-HMQC; natural abundance 14N reference

13C/15N enriched:

• cprfdr_20k.1p9 - C/C 2D exchange finite pulse RFDR; Vr=20kHz, mix 2.8ms reference cprfdr_20k
• cpdarr_20k.1p9 - C/C 2D exchange DARR for strong contacts; Vr=20kHz, mix 50ms reference cpdarr_20k
• cpdarr_13k.1p9 - C/C 2D exchange DARR longer distances (7.5A); Vr=13kHz, mix 200ms reference cpdarr_13k